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Die Coatings/Surface Treatment 
Task Group Guides R & D

Peter P Ried, Jr., Director Advanced Engineering
Doehler-Jarvis Technologies, Toledo, Ohio

Dr. Rajiv Shivpuri, Professor, Dept. of Industrial and Systems Engineering
The Ohio State University, Columbus, Ohio

The Die Coatings and Surface Treatment Task Group is chaired by Peter. P. Ried, Jr., Director, Advance Engineering, Doehler-Jarvis Technologies. This Task Group reports as a subcommittee to the NADCA Die Materials Committee. The mission of the task group is comprehensive:

  • To act as the coordinating entity and as the customer for research in die coatings and surface treatments for die casting applications
  • To monitor and guide contemporary research activity in this areas, to test and analyze the effectiveness of die coatings and surface treatments in the laboratory and on actual dies
  • To classify, model, and study coating and surface treatment types, coating/substrate system, and surface physical chemistry.
  • To evaluate prior research and develop a database on the coating application techniques, and use in die casting industry.
  • To disseminate qualitative and quantitative knowledge-based data on die coating and surface treatments and substrates.
  • To recommend specific die coating and/or surface treatment and substrate systems with appropriate die casting die manufacturing, care and usage guidelines to achieve the optimum combination of long life with low operating costs.

With these objectives in mind the task group is monitoring a DOE/NADCA sponsored project "Evaluation of Chromium Carbide and other PVD Coating to Improve the Wear Resistance of Aluminum Die Casting Dies." This project is being conducted at The Ohio State University with Dr. Rajiv Shivpuri, Prot~ssor, Department of Industrial and Systems Engineering, as the Principal Investigator. In the phase-I of the project (1995-96), the primary goal is to evaluate selected commercially available coatings, which have shown potential for wear resistance, in production scale tests and hence generate production scale data on the long term use (>100,000 shots) of coatings for the benefit of the die casting industry.

The industnal participation was in terms of providing beta test sites, sample coatings, heat treatment services, and steel test specimens. The phase-I project team consisted of die casting companies (Pace Industries, Inc., Doehler-Janis Pottstown), coating companies (Multi-Arc, Inc., Balzers Tool Coating, Arvin TD, Advance Heat Treat), heat treaters (FPM Heat Treatment) and steel suppliers Latrobe Steel).

Die selection was based on the following criteria, as defined by the industrial monitoring team:

  1. Die should have multiple cavities
  2. Die must have symmetry
  3. Die must be well known by the die easter and the process well established
  4. Local die process conditions known and documented near test feature
  5. Set-up frequency should be known
  6. Downtime causes must be documented in rank order of frequency
  7. Test core pin or insert geometry are well known

The tests were conducted on the basis of a randomized design. The objective of this design was to generate robust data (by blocking the influence of local variabilities such as difference in core pin attributes and flow conditions) which will permit it to be extended and applied to other dies. Candidate coatings were applied using Physical Vapour Deposition (PVD) and Therm-Reactive Deposition and Diffusion (TRD & D) method as described in Table 1.

Coatings were applied to core pins by participating coating companies according to their coating process specifications. The coated core pins were the put into production as per the experimental design. Periodic in-situ observation was carried out to monitor the coating performance.

For example, at one of the participating die casting companies, prior to the use of the coating, the cores were pulled out every 4 hr for cleaning the soldered material. This took on an average of 30 min, i.e. 1 hr per 8 hr shift. The life of the uncoated core pin was about 15,000 shots, after which the dies were disassembled and the cores replaced. The use of coated core pins completely eliminated the need for periodic cleaning of the cores and most of them lead to an increase in die life by more than 1Ox (127,500 shots) with significant saving in terms of machine downtime and labour of the order of $25,000 for one die. The fact that the cost of the coating was less than 10% of the savings made by the die caster, makes coating an economically viable solution to die wear problems.

The team also did substantial work on generation of fatigue data of coating/substrate combinations, conducted an extensive literature search on die coatings and an industrial survey on the use of die coatings. The literature search primarily focused on the coatings that are used in the die casting industry, the coating application technology and results obtained by laboratory and/or production tests. This document will be included as a part of the final report for the project report (due April 1997) which will form the basis for the database being built by the subcommittee.

The proposed phase-II (1997-99) of the project will focus on extending the current production scale evaluation to die inserts and die cavities of both multi-cavity and large single cavity dies. It will also address practical issues like repairability of dies, part ejection, effect of alloy composition and die heat treatment. One of the deliverables of the project will be to develop a comprehensive Design Methodology for the selection and use of coatings for extended die life.

The key benefits of participation in the proposed program will be:

  1. Extended die life by the use of wear resistant coatings
  2. Reduced die maintenance
  3. Reduced machine downtime
  4. Reduced labor costs
  5. Access to generated knowledge-based information

The task group solicits participation from die casters, coating suppliers, heat treater, and steel suppliers in the proposed phase-II program. Involvement in and contributions to the Die Coatings and Surface Treatment Task Group may take one or more of several forms. These include:

  1. funding research directly,
  2. providing technical direction and oversight through the Task Group, and
  3. executing a systematic testing program and tracking plan, providing failed pins along with relevant background data in cooperation with the Principal Investigator.

If your company is interested in participating, please contact:

Mr. Peter Ried, Chair, Die Coating and Surface Treatment Task Group
T: 419.470.8170
F: 419.470.8185

or Dr. Rajiv Shivpuri
T: 614.292.7874
F: 614.292.7852

Table 1: Coating materials and processes

Published in January/February 1997/41 issue of
North American Die Casting Association Joumal.

 

 


NOTES ON THE MEETING OF NADCA DIE COATINGS AND SURFACE TREATMENT TASK GROUP
October 3, 1997 - Ohio State University, Columbus, OH

Long Range objectives of research:

reduce soldering 10 to 20 times
reduce surface lubrication 30 to 50%
reduce casting ejection distortions 50%
reduce ejection forces 50%
improve net shape capability 20 to 30%
reduce scrap 25 to 50%
reduce die repair expenses 50 to 85%

Participants:

  • Doehler-Jarvis Technologies
  • DCD Technologies
  • Eastern Alloys
  • Patterson Mold
  • Advanced Heat Treat
  • Balzers Tool Co.
  • General Die Casters
  • Ganton Technologies
  • GM Powertrain
  • Saint Clair Die Casting
  • Anderson Die Casting
  • Arvin TD
  • Multi Arc
  • Tool Products
  • Contech
  • Ahresty
  • Alcoa
  • R.B. Alexander & Assoc
  • Sun Steel Treating
  • Diltech/Dynacast
  • Maytag
  • DuPage Die Casting
  • Oak Ridge National Laboratory
  • CMI Tech Center
  • CMI Precision Mold
  • Briggs & Straton
  • Muskegon Castings
  • Chem Tren
  • Perf. Engineering Coatings
  • Sputtek Inc.
  • Badger Metal
 

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